集成光学器件的PLZT薄膜溶胶-凝胶法制备与性能研究
DOI:
CSTR:
作者:
作者单位:

作者简介:

崔一平(1957-),男,江苏海安人,博士,教授,博士生导师 ,主要从事纳米光电功能材料、器件与应用、光通信与光集成传感技术等研究方向.

通讯作者:

中图分类号:

基金项目:

国家自然科学基金(60907025)资助项目 (东南大学 电子科学与工程学院,江苏 南京 210096)


Fabrication and characterization of PLZT thin films prepared by sol-gel method for integrated optical devices
Author:
Affiliation:

Fund Project:

  • 摘要
  • |
  • 图/表
  • |
  • 访问统计
  • |
  • 参考文献
  • |
  • 相似文献
  • |
  • 引证文献
  • |
  • 资源附件
  • |
  • 文章评论
    摘要:

    在掺铌钛酸锶(NST)的衬底上, 通过加入抑制开裂剂聚乙二醇对异辛基苯基醚(triton X-100), 利用溶胶-凝胶法制备了厚达4.6μm的 锆钛酸铅镧(PLZT)薄膜,从而有效地减小了其在集成光学器件应用中的传输损耗。实验分析 了triton X-100的加入量对薄膜质量的影响,并通过优化triton X-100的加入量可有效抑制薄 膜开裂。利用光学显微镜、扫描电子显微镜(SEM)、X射线衍射仪(XRD)、棱镜耦合波导 测试仪和台阶 仪等对制备的薄膜性能进行分析。结果表明,经过650℃快速退火处 理后,得到了表面平整度小于30nm、 粒径为50~100nm的钙钛矿结构PLZT薄膜,测得PLZT(8/65/35)和PL ZT(11/65/35)薄膜在 1550nm波长处的折射率分别为2. 4029和2.388。本文方法制备的 薄膜可以用于PLZT电光器件的制作。

    Abstract:

    PLZT films have many significant applications in the field of integrat ed optics because of their desirable physical properties,such as dielectric properties,electric-optic eff ect and polarization insensitivity.A certain thickness of the electro-optic film is needed in the ap plication of integrated optical devices.Currently,it is hard to obtain more than 3μm PLZT thin film,because th e film is very easy to crack as the process is repeated for several times and the high-temperature annealing treatm ent is taken during the fabrication of PLZT thin film by sol-gel methods.In this paper,a 4.6μm thick PLZT thin fil m was fabricated on Nb-doped strontium titanate (NST) substrate using sol-gel methods by adding tr iton X-100as the stress crack inhibitor in order to reduce the propagation loss in the applications of i ntegrated optical devices effectively.The effect of the added amount of triton X-100on the film propert y is studied experimentally. And the film cracking can be eliminated effectively by optimizing the triton X -100amount.Meanwhile, the obtained film is characterized by optical microscope,scanning electron mic roscopy (SEM),X-ray diffraction (XRD),prism coupler and step profiler.The results show that the pe rovskite PLZT film is obtained after rapid thermal annealing at 650℃ for 30min,and the flatness of the film surface is less than 30nm with the average particle size of 50-100nm.The measured refractive indices of the PLZT (8/65/35) and the PLZT (11/65/35) films are 2.4029and 2.3885,respectively at the wavelength of 1550nm.They can both be used for PLZT e lectro-optical device fabrication.

    参考文献
    相似文献
    引证文献
引用本文

杨柳,胡国华,恽斌峰,章丽昕,崔一平.集成光学器件的PLZT薄膜溶胶-凝胶法制备与性能研究[J].光电子激光,2013,(12):2338~2343

复制
分享
文章指标
  • 点击次数:
  • 下载次数:
  • HTML阅读次数:
  • 引用次数:
历史
  • 收稿日期:2013-04-07
  • 最后修改日期:
  • 录用日期:
  • 在线发布日期:
  • 出版日期:
文章二维码